| Identification | Back Directory | [Name]
4,5-Dibromo-3-methylthiophene-2-carboxylic acid | [CAS]
854626-32-7 | [Synonyms]
4,5-dibromo-3-methyl-2-Thiophenecarboxylic acid
4,5-Dibromo-3-methylthiophene-2-carboxylic acid | [Molecular Formula]
C6H4Br2O2S | [MOL File]
854626-32-7.mol | [Molecular Weight]
299.97 |
| Hazard Information | Back Directory | [Preparation]
4,5-Dibromo-3-methyl-2-thiophenecarboxylic acid synthesis: 4,5-dibromo-3-methyl-2-thiophenecarbonitrile (26.2 g, 92.2 mmol), EtOH (175 mL), water (175 mL), and NaOH (18.6 g, 466 mmol) were stirred together at 80°C for 1 h. The solvent was removed, the solids were collected by filtration, dissolved in water, and washed with CH2Cl2. The water layer was acidified with 37% HCl, the white solid was collected by filtration and dried under vacuum at 60°C to give 25.9 g (94% wt.) of 4,5-dibromo-3-methyl-2-thiophenecarboxylic acid: m.p. 225-226°C; 1H NMR (CDCl3) 2.5 (s). |
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| Company Name: |
BePharm Ltd
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| Tel: |
400-685-9117 |
| Website: |
www.bepharm.com |
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