Identification | Back Directory | [Name]
4-oxopiperidinium chloride | [CAS]
41979-39-9 | [Synonyms]
Nsc134482 4-Piperidone Hcl PIPERIDIN-4-ONE,HCL 4-oxopiperidinium chloride 4-oxyperidone hydrochloride 4-Piperidinone hydrochloride 4-Oxopiperidine hydrochloride 6-Fluorospiro[chroman-2,4' Piperidine-4-one·hydrochloride Piperidin-4-one hydrochloride 95% 4-Piperidinone,hydrochloride (1:1) 4-Oxopiperidinium chloride hydrochloride 4-Piperidinone Hydrochloride
DISCONTINUED | [EINECS(EC#)]
255-602-8 | [Molecular Formula]
C5H10ClNO | [MDL Number]
MFCD00041019 | [MOL File]
41979-39-9.mol | [Molecular Weight]
135.592 |
Questions And Answer | Back Directory | [Physical Form]
White to yellow solid | [synthesis]
To a solution of tert-butyl 4-oxopiperidine-1-carboxylate (2300 g, 11.6 mol) in 1,4-dioxane was added a solution of HCl (g)/1,4-dioxane (4 L, 10 mol/L) slowly at 0°C. After the addition, the reaction mixture was stirred for 4 h and TLC (EtOAc/petroleum ether = 1:5) showed the reaction was complete. The solvent was removed in vacuo to afford piperidin-4-one hydrochloride as a brown solid.
Fig The synthetic method of 4-oxopiperidinium chloride |
|
|