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ChemicalBook--->CAS DataBase List--->3278-89-5

3278-89-5

3278-89-5 Structure

3278-89-5 Structure
IdentificationBack Directory
[Name]

2-Allyloxy-1,3,5-tribromobenzene
[CAS]

3278-89-5
[Synonyms]

DXFR? 401
ALLYL TRIBROMOPHENYL ETHER
TRIBROMOPHENYL ALLYL ETHER
2-allyloxy-1,3,5-tribromobenzene
ALLYL 2,4,6-TRIBROMOPHENYL ETHER
2,4,6-Tribromophenyl allyl ether
1-(Allyloxy)-2,3,4-tribromobenzene
1,3,5-tribromo-2-prop-2-enoxybenzene
Allyl 2,4,6-tribromophenyl ether 98%
1,3,5-tribromo-2-prop-2-enoxy-benzene
1,3,5-tribromo-2-(2-propenyloxy)-benzen
Benzene,1,3,5-tribromo-2-(2-propenyloxy)
1,3,5-TRIBROMO-2-(2-PROPENYLOXY)-BENZENE
1,3,5-TribroMo-2-(2-propen-1-yloxy)-benzene
Benzene, 1,3,5-tribromo-2-(2-propen-1-yloxy)-
2,4,6-Tribromophenyl allyl ether @100 μg/mL in Toluene
[EINECS(EC#)]

221-913-2
[Molecular Formula]

C9H7Br3O
[MDL Number]

MFCD00017773
[MOL File]

3278-89-5.mol
[Molecular Weight]

370.86
Chemical PropertiesBack Directory
[Melting point ]

74-76 °C (lit.)
[Boiling point ]

339.5±37.0 °C(Predicted)
[density ]

1.950±0.06 g/cm3(Predicted)
[EPA Substance Registry System]

Allyl 2,4,6-tribromophenyl ether (3278-89-5)
Safety DataBack Directory
[WGK Germany ]

3
Hazard InformationBack Directory
[Application]

1,3,5-Tribromo-2-(2-propen-1-yloxy)-benzene is used as a brominated flame retardant.
Not a dangerous good if item is equal to or less than 1g/ml and there is less than 100g/ml in the package.
[Synthesis]

Synthesis_3278-89-5
To the ethanol solution of the sodium tribromophenolate salt prepared in the step 1), the dispersing agent sodium stearate 2.5 g is added.And catalyst II phenyl triethyl ammonium chloride 5.6g,The temperature is raised to 75 ?? C to reflux the reaction.Further, 1000 ml of an ethanol solution of chloropropene having a volume ratio of chloropropene to ethanol of 1:5 was slowly added thereto, and then the reaction was kept at 75 ?? C for 6.5 h until the end.Then, the temperature is lowered to 7 ?? C in sequence, and then suction filtration is performed to recover the ethanol solution.After washing the filter cake with water, the filter cake was dried at 60 ?? C.2,4,6-Tribromophenyl allyl ether was obtained as a white powdery solid in a yield of 96.2%.
Spectrum DetailBack Directory
[Spectrum Detail]

2-Allyloxy-1,3,5-tribromobenzene(3278-89-5)IR
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