Identification | Back Directory | [Name]
2-Allyloxy-1,3,5-tribromobenzene | [CAS]
3278-89-5 | [Synonyms]
DXFR? 401 ALLYL TRIBROMOPHENYL ETHER TRIBROMOPHENYL ALLYL ETHER 2-allyloxy-1,3,5-tribromobenzene ALLYL 2,4,6-TRIBROMOPHENYL ETHER 2,4,6-Tribromophenyl allyl ether 1-(Allyloxy)-2,3,4-tribromobenzene 1,3,5-tribromo-2-prop-2-enoxybenzene Allyl 2,4,6-tribromophenyl ether 98% 1,3,5-tribromo-2-prop-2-enoxy-benzene 1,3,5-tribromo-2-(2-propenyloxy)-benzen Benzene,1,3,5-tribromo-2-(2-propenyloxy) 1,3,5-TRIBROMO-2-(2-PROPENYLOXY)-BENZENE 1,3,5-TribroMo-2-(2-propen-1-yloxy)-benzene Benzene, 1,3,5-tribromo-2-(2-propen-1-yloxy)- 2,4,6-Tribromophenyl allyl ether @100 μg/mL in Toluene | [EINECS(EC#)]
221-913-2 | [Molecular Formula]
C9H7Br3O | [MDL Number]
MFCD00017773 | [MOL File]
3278-89-5.mol | [Molecular Weight]
370.86 |
Hazard Information | Back Directory | [Application]
1,3,5-Tribromo-2-(2-propen-1-yloxy)-benzene is used as a brominated flame retardant. Not a dangerous good if item is equal to or less than 1g/ml and there is less than 100g/ml in the package. | [Synthesis]
To the ethanol solution of the sodium tribromophenolate salt prepared in the step 1), the dispersing agent sodium stearate 2.5 g is added.And catalyst II phenyl triethyl ammonium chloride 5.6g,The temperature is raised to 75 ?? C to reflux the reaction.Further, 1000 ml of an ethanol solution of chloropropene having a volume ratio of chloropropene to ethanol of 1:5 was slowly added thereto, and then the reaction was kept at 75 ?? C for 6.5 h until the end.Then, the temperature is lowered to 7 ?? C in sequence, and then suction filtration is performed to recover the ethanol solution.After washing the filter cake with water, the filter cake was dried at 60 ?? C.2,4,6-Tribromophenyl allyl ether was obtained as a white powdery solid in a yield of 96.2%. |
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