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ChemicalBook--->CAS DataBase List--->326-43-2

326-43-2

326-43-2 Structure

326-43-2 Structure
IdentificationBack Directory
[Name]

alpha-[(2-pyridylamino)methyl]benzyl alcohol monohydrochloride
[CAS]

326-43-2
[Synonyms]

Vazalmin
Firmalgil
Phenyramidol HCl
FENYRAMIDOLHYDROCHLORIDE
alpha-[(2-pyridylamino)methyl]benzyl alcohol monohydrochloride
[EINECS(EC#)]

206-308-3
[Molecular Formula]

C13H15ClN2O
[MDL Number]

MFCD00242757
[MOL File]

326-43-2.mol
[Molecular Weight]

250.724
Chemical PropertiesBack Directory
[Melting point ]

140-142°
Safety DataBack Directory
[Symbol(GHS) ]


GHS07
[Signal word ]

Warning
[Hazard statements ]

H302-H315-H319-H335
[Precautionary statements ]

P261-P280-P301+P312-P302+P352-P305+P351+P338
[Toxicity]

LD50 oral in mouse: 2425mg/kg
Hazard InformationBack Directory
[Originator]

Analexin, Mallinckrodt Inc., US ,1960
[Uses]

Analgesic; relaxant (skeletal muscle).
[Manufacturing Process]

A mixture containing 188 g (0.20 mol) of 2-arninopyridine, 0.55 g of lithium amide and 75 cc of anhydrous toluene was refluxed for 1.5 hours. Styrene oxide (12.0 g = 0.10 mol) was then added to the reaction mixture with stirring over a period of ten minutes. The reaction mixture was stirred and refluxed for an additional 3.5 hours. A crystalline precipitate was formed during the reaction which was removed by filtration, MP 170°C to 171°C. 1.5 g. The filtrate was concentrated to dryness and a dark residue remained which was crystallized from anhydrous ether; yield 6.0 g. Upon recrystallization of the crude solid from 30 cc of isopropyl alcohol, 2.0 g of a light yellow solid was isolated; MP 170° to 171°C.
[Therapeutic Function]

Analgesic, Muscle relaxant
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