| Identification | Back Directory | [Name]
2-(4-CHLOROBUTYL)-1,3-DIOXOLANE | [CAS]
118336-86-0 | [Synonyms]
2-(4-CHLOROBUTYL)-1,3-DIOXOLANE
1,3-Dioxolane,2-(4-chlorobutyl)-
5-CHLORO-N-VALERALDEHYDE ETHYLENE ACETAL | [Molecular Formula]
C7H13ClO2 | [MDL Number]
MFCD00043136 | [MOL File]
118336-86-0.mol | [Molecular Weight]
164.63 |
| Chemical Properties | Back Directory | [Boiling point ]
56-58 °C/0.1 mmHg (lit.) | [density ]
1.109 g/mL at 20 °C (lit.) | [refractive index ]
n20/D 1.457
| [Fp ]
85 °C | [storage temp. ]
Inert atmosphere,2-8°C | [BRN ]
4304948 |
| Hazard Information | Back Directory | [Uses]
2-(4-Chlorobutyl)-1,3-dioxolane was used in the synthesis of C-chlorobutylpyrogallol[4]arene. | [Purification Methods]
If the IR has no CHO band, then just distil it in a vacuum. If it is present, then dissolve it in Et2O, wash it with H2O, then saturated NaHCO3, dry over MgSO4, evaporate and distil it. [cf Kriesat & Gisvold J Pharm Sci 60 1250 1971, Loftfield J Am Chem Soc 73 1365 1951.] |
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