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ChemicalBook--->CAS DataBase List--->10213-09-9

10213-09-9

10213-09-9 Structure

10213-09-9 Structure
IdentificationBack Directory
[Name]

vanadium dichloride oxide
[CAS]

10213-09-9
[Synonyms]

Vanadyl dichloride
VANADYLOXYCHLORIDE
dichlorooxovanadium
dichlorooxo-Vanadium
VANADYLOXYDICHLORIDE
Vanadium oxydichloride
Vanadium, dichlorooxo-
Dichlorooxovanadium(IV)
Vanadium(IV) oxychloride
vanadium dichloride oxide
oxovanadium,dihydrochloride
Vanadium(IV) dichlorideoxide
Vanadium(IV) oxidedichloride
Vanadium(IV) dichloride oxide
[EINECS(EC#)]

233-517-7
[Molecular Formula]

Cl2OV+
[MDL Number]

MFCD00011458
[MOL File]

10213-09-9.mol
[Molecular Weight]

137.847
Chemical PropertiesBack Directory
[density ]

2.88
[solubility ]

reacts with H2O; soluble in ethanol
[form ]

green hygroscopic crystals
[color ]

green hygroscopic crystals, crystalline
[Water Solubility ]

slowly decomposed in water; soluble absolute alcohol, glacial acetic acid [MER06]
[EPA Substance Registry System]

Vanadium, dichlorooxo- (10213-09-9)
Hazard InformationBack Directory
[Chemical Properties]

Green, deliquescent crystal. Usual technical product is a dark-green, syrupymass, 76–82% pure, or a solution. Slowly decomposed by water; soluble in water, alcohol, and acetic acid; may react violently with potassium.
[Uses]

Has been used as mordant in printing fabrics.
[Hazard]

Strong irritant to tissue.
[Preparation]

A thoroughly ground mixture of 3.6 g. of dry V2O5 and 9.4 g. of VCl3 is placed at the closed end of a l-m.-longtube, and 0.9 ml. of VOCl3 is then added. The upper part of the tube must be free of traces of these substances. The tube, filled with air, is melt-sealed, and is covered along its entire length with a sheet-metal jacket; its lower third, in a slightly inclined position, is then heated to about 600℃ with a tubular electric furnace. The sheet-metal jacket provides a temperature gradient along which the product VOCl2 sublimes out of the hot reaction zone. This procedure requires at least 4-5 days. However, the yield can be increased by longer heating time. Green needlelike crystals of VOCl2 are deposited in the cold part of the tube. The tube is opened at a suitable spot; the product is suspended in petroleum ether, ethyl ether or CCl4 to dissolve some adhering VOCl3, and then suction-filtered on a coarse fritted-glass filter. The relatively coarse filter separates the VOCl2 crystals from traces of finely divided hydrolysis products. The VOCl2 is freed of adhering solvent and stored under anhydrous conditions.preparation of vanadium dichloride oxide
Safety DataBack Directory
[Symbol(GHS) ]


GHS07,GHS05
[Signal word ]

Danger
[Hazard statements ]

H302-H314
[Precautionary statements ]

P260-P264-P280-P301+P330+P331-P303+P361+P353-P363-P304+P340-P310-P321-P305+P351+P338-P405-P501-P264-P270-P301+P312-P330-P501
[RIDADR ]

2923
[HazardClass ]

8
[PackingGroup ]

III
Spectrum DetailBack Directory
[Spectrum Detail]

vanadium dichloride oxide(10213-09-9)IR1
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