Identification | Back Directory | [Name]
4-Amino-2-fluoro-5-methoxybenzoic acid | [CAS]
1001346-91-3 | [Synonyms]
4-Amino-2-fluoro-5-methoxybenzoic acid Benzoic acid, 4-amino-2-fluoro-5-methoxy- 4-Amino-2-fluoro-5-methoxybenzoic acid USP/EP/BP | [Molecular Formula]
C8H8FNO3 | [MDL Number]
MFCD11849929 | [MOL File]
1001346-91-3.mol | [Molecular Weight]
185.15 |
Hazard Information | Back Directory | [Synthesis]
A solution of 2-fluoro-5-methoxy- 4-nitrobenzoic acid (10 g, 46 mmol), HOAc (50 mL), and MeOH (50 mL) was hydrogenated using a hydrogen balloon overnight. The solution was then filtered through celite and concentrated to a residue, which was triturated with ether and ethyl acetate. The solid was filtered and dried to give the product 4-Amino-2-fluoro-5-methoxybenzoic acid as a light yellow powder (8.3 g, 98 %).
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